removing methanol from applejack

So... you can't hold it at the boiling point of one compound and get just that compound. Be more wary of methanol when distilling fruits, as opposed to sugar washes, grain washes, or whiskeys. Found insideThis book is for all of us who appreciate Mother Nature's creatures, no matter how humble. After freezing the applejack, you can eliminate the methanol by warming the jack to about 150 to 160 degrees F. Use a thermometer. I'm excited to get started and wish you the best of luck. I need to figure out how much brown sugar to add to one gallon of cider, the Super yeast is supposed to have that info on the package. Tall grass, weeds, and bushes allow mosquitoes protection from the midday sun. APPLE JACK FROZEN HARD CIDER DANGER DANGER ok when you cryogenically remove the water (freeze it), you concentrate the ethanol, AS WELL AS THE METHANOL. Boiling it at 78 and collecting it would give you both ethanol and methanol. No pectic. The Applejack Sour uses 1/2 a lime and 1/2 a lemon along with Grenadine and powdered sugar. I don’t have the answer for you but I say it is worth a try. It's not a concern in the least with making Applejack. Methanol boils at about 150 whereas the ethanol doesn't boil till about 170. . After freezer-distilling Applejack could I theoretically heat up the distillate in an open pot to around 148F for a couple min and just "boil off" some of the methanol? You must log in or register to reply here. Removing the Methanol. I'm not saying what you make isn't going to give you a hangover, but it isn't going to be from methanol. Be ruthless about tossing the first 50 mL (off a 20L wash) that you collect, as this contains any methanol (causer of hangovers - small quantities, or blindness - larger quantities). Methanol is POISON or in smaller quantities, very TOXIC. So a week in, you froze your hard cider twice to make apple jack? The reasoning behind Methanol in home distillation is related back to the prohibition era. Nobody showers with boiling water. Type 3A is what is commonly used to dry ethanol and methanol. There is only 5 ounces of alcohol in a gallon, and it will not come out w/o a significant amount of the water/cider with it. The dog was ethylene glycol. Then Report back. Meet the all-new Hypersoft Sneakers. shut off the still, and transfer out through a counter flow chiller to reduce time at temp, and O2 exposure. Freeze distillation can concentrate methanol and fusel alcohols (by-products of fermentation which true distillation separates out) in applejack to unhealthy levels. To start with, that's not how boiling mixtures works. No, your idea wouldn't work, due to azeotropes and whatnot. Divided into five parts, this comprehensive two-volume work presents: INTRODUCTION, BACKGROUND AND HISTORY: A simple introduction to the history and development of alcohol and some recent trends and developments, FERMENTED BEVERAGES: BEERS, ... DIRECTIONS. Methanol boils at 65 so this should get rid of methanol and not ethanol. There are links explaining this in the thread I posted. After this, drain the top liquid layer and remove the sediment at the bottom. . If you do some science, keep notes and keep some as it was to compare. Apples are among the most popular fruits in the world. (b) The food additive meets the following specifications: (Where methods of determination are specified, they are Association of Official Analytical Chemists Methods, 13th ed., 1980, which . Apple seeds actually have a chemical that turns into trace amounts of cyanide so we prefer to remove the seeds before processing. ET on Wednesday, the unofficial COVID-19 tally in the U.S. reached 26,436,594 cases and 446,901 deaths -- up 114,229 and 3,288, respectively, from Tuesday. Sure you could absolutely do that. The jacking, or freeze distillation process had a dangerous byproduct: Methanol. -100 lbs of oil + 10 lbs of methanol -> 100 lbs of biodiesel + 10 lbs of glycerol •Bioethanol -An alcohol made by fermenting sugars from biological materials (starch crops --corn) or cellulosic biomass (trees, grasses) -Can be used as vehicle fuel in its pure form or as a gasoline Methanol, at too high of quantities, results in blindness or death. Applejack gets its name from the process and ingredients that are used in its production. Found insideThis volume features an extra focus on the conceptual design of distillation. And they like it. heat to boiling, take off your fores, and even heads. You cannot selectively remove methanol by maintaining the boiling temperature of pure methanol. It's much higher in apple juice than beer. If your looking to make cheap shit to get everybody drunk I'd recommend making some welches grape wine and carbonate it, just use the frozen cans of concentrate, water, sugar, champagne yeast. It will, but it doesn't change the ratio of ethanol to methanol, so my point stands. Smoke extractor or at least a fan pointing out a window to draw out the vapors would be a good idea. Apparently super yeast makes bad tastes (fusel alcohols?) Add 8-10 grams of baking soda per 1 liter of moonshine, stir, and infuse for 20-30 minutes. Flesh firmness of Pink Lady apple was generally higher when . Traditional applejack made by freezing multiple times and removing the ice each time concentrates the bad alcohols and other crap (methanol and fusel alcohol) that are removed in distillation. 3 nmol/cm2) calculated from the equation with methanol, acetone, and with the Folch system (see Ma- terials and Methods) A ( λ ) = A 0 ( λ ) - [ ε α ( λ )C a + ε b ( λ )C b ], (1) The fraction of extracted pigments, % where A(λ) is the . Applejack (drink) Applejack is a strong alcoholic drink produced from apples. The H/C ratio for ethanol is slightly smaller (H/C = 3) than that of methanol (H/C = 4), hence I would expect that ethanol would burn with a somewhat more yellowish fl. The sample preparation process for the removal of residual solvents is shown in Fig. It is the rapid polymerisation of o-quinones to produce black, brown or red polyphenolic pigments that is the cause of fruit browning. I made applejack for my bachelor party coming up, and it has been successful so far. Found insideFrom "spirited" camp meetings, to bourbon's use as a medium of exchange for goods and services, to the industry's coming of age in the mid-nineteenth century, the story of Kentucky bourbon is a fascinating chapter in the state's early ... Fun projects and valuable content join forces to enable readers to turn their wireless home network into a high-performance wireless infrastructure capable of entertainment networking and even home automation Step-by-step instructions help ... immersing the material in methanol and subsequent ultrasonification. I'm asking for a good recipe for back sweetening besides white sugar. This encyclopedia presents the many sides of America's ongoing relationship with alcohol, examining the political history, pivotal events, popular culture, and advances in technology that have affected its consumption. • More than 100 ... Methanol is a poison to humans or will at least make them very sick. siphon your applejack into the still and then fill the column with a couple of busts of CO2 in order to reduce O2 exposure. Molasses? You can remove the methanol simply by steeping your finished product for for a . The steam coming off a heated open pot of liquid will be a mixture of everything in that pot. I thought apple jack didn't need back sweetening, but I'm thinking about doing it to cover the tartness. I'd bring it just to the solution's boiling point in an open pot... let it sit there for 2 minutes.... then put the pot lid on top and turn off the heat. distiller blow off the first 7% or so of a run, as it is METHANOL (that is the header), they then continue the run and at some point stop . Making apple jack out of a 4-5% ABV cider is going to be difficult at best. If you're up to some other sorcery, I have nothing to offer. Ethanol and Methanol are essentially impossible to separate by distillation. Joined: Mon Apr 12, 2010 5:39 am. I used to make 5 gal at a time and keg carbonate it once it settled out, made for good house parties and wine pong and it tastes a shitton better than apple wine, even if it isn't great. I can tell you from personal experience that the hangovers from apple jack (and shitty apple juice wine) are gonna be gnarly. You'd die of alcohol poisoning long before the methanol kicked in. I guess theres nothing to be worried about... only thing left to do is drink! I plan to freeze distill. TLDR methanol in cider or in jacked cider is not more of a health concern than the ethanol is. Applejack and apple-infused brandy are liqueurs that you can make at home with a little bit of effort and a lot of patience. Found insideMATLAB is an indispensable asset for scientists, researchers, and engineers. Popular in the American colonial era, the drink's prevalence declined in the 19th and 20th centuries amid competition from other spirits. Specialty, Fruit, Historical, Other Recipes, http://www.while-science-sleeps.com/pdf/141.pdf, http://www.dailymail.co.uk/news/art...ves-puppy-poisoned-anti-freeze-Australia.html, The "I'd nevervdrink that if it were ALL that was available" thread. Janik grew up surrounded by apple iconography in Washington, the “apple state,” so there is no better author to tell this fascinating story. To my experience you cannot differentiate between burning ethanol and methanol. Soxhlet extraction with methanol. which are also made without a distillation step. In order to optimize conditions for the extraction of polyphenols from apples, peel and flesh of apples were subjected to an extraction process with different solvents consisting of various ratios of methanol and water (40, 60, 80 %), 100 % methanol, or with methanol acidified with hydrochloric acid (0.1 %). (4) The additive shall be prepared by extraction with hexane and food-grade ethanol to remove fat and moisture. I wanted sweet, not tart. Applying different extraction techniques it is possible to . Flavonoids are one of the main groups of polyphenols found in natural products. Found insideIn addition to the current terminology of every component of pastry, baking, and confectionary arts, this book provides important information about the origin and historical background of many of the terms. releases methanol when broken down by the body which is a toxic substance . As for the brown sugar, you really can add as much as you like, but if you end up adding quite a bit, I would recommend adding it in smaller increments so you don't strain the yeast too bad. That will mess you up. Charlotte - removing methanol and acetone from drinks is an advantage of distilling over drinking fermented drinks without distilling (though we still do that all the time, hence this group) but it's also worth mentioning that the capability for amateur distillers to separate methanol from its antidote is a potential source of danger too . Read the Applejack discussion from the Chowhound Spirits, Applejack food community. Not at all. Share techniques, equipment, still designs, recipes, materials sources, and anything related to beverage distillation. If that weren't true, you'd see pages and pages of people telling you how to turn denatured alcohol back into 190 proof ethanol. Nope. Purified paclitaxel (purity: 98.7%) was obtained by drying of pooled fractions at 35 °C under reduced pressure. Press question mark to learn the rest of the keyboard shortcuts. The apple's natural wax is washed off when removing pesticide residue so bees wax is added to apple to prevent it from going bad. Found insideOut of Line describes Lynch’s remarkable process of self-invention, including her encounters with colorful characters of the food world, and vividly evokes the magic of creation in the kitchen. apples in particular, does yield a small amount of methanol. In the case of 3A, the spaces are 3 angstroms. In this episode I make a traditional spirit that dates back to early colonial America. How many apples do I need to make cider? I think its vinegar bacteria that causes that, am I right? You should also avoid saturated fats, like cheese, butter and margarine. That actually MIGHT reduce some of the nail-polishy heads stuff. This guide to the language differences between the United States and United Kingdom is “a fascinating collection full of all kinds of surprises” (Minneapolis Star Tribune). The design of the sample flow path in the autosampler, features controlling needle washing, and the chemistry of the wash solvent all play a role in eliminating detectable carryover. In an updated encyclopedic study of the history and uses of psychoactive plants and related substances, the author offers a blend of authority and playfulness and includes a new introduction to each resource. How to Remove Methanol from Moonshine. The fiber helps to absorb the crystals, removing them from your joints and helping to eliminate them from your kidneys. We used a mixture: about 20 pounds of Gala, 4 pounds of Granny Smith, and 2 pounds (or so) of Honey Crisp. When you are happy with the infusion, strain the vodka into a fresh jar and discard the apples. In a large pot, combine apple juice, apple cider, sugar and cinnamon sticks. Make sure you are outdoors or at least in a well ventilated area and keep up wind of the vapors. Removal of the solvent in vacuum will yield a crude material with significant amounts . So what to do? This manual describes, at the craft level, the process of making whiskey. I would bet that as OP guessed warming it to the right temperature would remove a good bit of the methanol but I don't know what else might be lost or what other changes might happen in the remaining product. The word "jack" derives from the process of freeze distillation, which has historically been called "jacking." Applejack was/is commonly distilled from apple cider. Youlle never get to a danger zone with freezing. Lactose will add mouth feel a little thicker on the tongue. A comprehensive home-distilling book that specifically addresses the small-scale production of whiskey. The whole TTB thing with home distillation is a fallacy, it's more of an excuse for excise taxes than it is a public safety concern. Extractions were performed using an ultrasonic bath with time periods from 5 to 15 min . The first step in correcting a moldy wine is diagnosis -- you can sometimes save a wine if you identify the type of mold and treat it accordingly. There should never be any methanol (wood alcohol) in wine that a human consumes. Furthermore if you process 1000 pounds per day, this would be your daily loss. It is a type of fruit brandy . Eurytrema will not settle and multiply in our pancreas without the presence of wood alcohol (methanol). I ordered a 1 gallon glass fermenter and a pack of super yeast that says it will get the alcohol content up to 20%. "The Origins of Chemistry" integrates the histories of Greek, Arabic, and Latin alchemical traditions with philosophy, technology, and the genesis of medical chemistry. If you are helping other people remove their clothing, try to avoid touching any contaminated areas, and remove the clothing as quickly as possible. Due to osmotic pressure water (and whatever else is smaller than 3 angstroms) is essentially forced into the sieve. For Cider Clarity - Add pectic enzyme / pectinase (optional) Pectic enzyme can be added to reduce haze and improve the clarity of the final cider; however, it's also been shown that adding pectic enzyme can increase the methanol level in the final brew (though it's generally thought that the amount of methanol released from apples during fermentation is too small to matter). However: You might want to try molecular sieves. Do this outside, or in a fume hood. The boiling point of methanol is 148°F (64.7°C) so if you want to boil it off before the Ethanol, boiling point 173°F (78.37°C) you could do that. Recipe was 10 cans frozen apple juice concentrate and 8 pounds of dark brown sugar (5 gallons initially), fermented with Red Star Champagne Yeast at 70°F. Kept up to date with supplements between editions 1977- prepared by U.S. Dept. of Commerce, Office of Federal Statistical Policy and Standards. You'd essentially be taking a heads cut, without bothering to collect it. Made especially for women's feet with a patented three-way Orthotic Arch Support System that makes every step comfortable and powerful. I'm not sure removing the heads without removing the tails would be worth it to me... but... it's not impossible that he might change the character of what he's making for the better, is it? Found inside – Page 1This book is a backstage pass into the world of small-scale distilling of whiskies, gins, vodkas, brandies, and more. . Put it in a pan with a thermometer and heat it to about 68-72. YES - the most volatile compounds come off in the greatest concentration first... but from the first drop to the last you're getting SOME of everything. Infuse your moonshine with orris root for 12 days (100 . So, if you want to fill your traditional 23 beer fermenter, do the maths and you'll find you need 46 kgs of apples. In insects, PPO serves for the cuticle hardening. Then stir again and leave for 10-12 hours. 1 gallon apple cider. Soda is good for getting rid of fusel oils that cause an unpleasant smell. And explain why you shouldn't make it because of the health risks associated drinking Applejack. Lairds which is the only maker of something called applejack in the US distills it and in actuality it is a apple based spirit. The three fruits had a very good antioxidant activity. Sometimes the applejack would be charcoal filtered to remove impurities and aged like whiskey in oak barrels. When it comes to the smoothest, most expensive, top-shelf vodka brands in the world, we've rounded up the 15 best vodkas at every price. shut off the still, and transfer out through a counter flow chiller to reduce time at temp, and O2 exposure. Wait... did you add methanol to your applejack? Found insideFirst published in 2005. Routledge is an imprint of Taylor & Francis, an informa company. I have stabilized, but didn't back sweeten yet. Found insideWith editors and contributors from 24 countries in North America, Europe, and Asia, this guide provides international expertise and a truly global perspective on food manufacturing. Even in distilleries, they aren't dropping the heads and tails because of methanol, it's due to fusel oils that you don't want in your dram. It is made by freezing the cider and removing the ice crystals that form. You still don't have enough methanol to worry about. I racked and froze the juice twice. The other thing could be your freezer, what temperature is it set to? The American Spirit Isn't this fundamentally true for any fermented thing that one might later distill? The reasoning behind Methanol in home distillation is related back to the prohibition era. You have to go to the solution boiling point. Sarah made some delicious apple scrap cake after juicing our apples! The best way is to not worry about it and drink it. Do yourself a favor and buy a real still and make some schnapps from it if you really want to make strong apple based stuff, they drink loads of this in germany and it's great. That will mess you up. Removing the water changes the Alcohol freezes at a much lower temperature than water, so it remains in a liquid state. Remove methanol and kojic acid source; Zapping; Remove Pfloridzin, a food allergen All diabetics have a common fluke parasite, Eurytrema pancreaticum, the pancreatic fluke of cattle, in their own pancreas. Found insideWith more than 900 entries of everything from "Abbey Beer" to "Zymurgy," and hundreds of illustrations, this book answers all your questions on: - influential brewers and their products - beer styles--both the popular and the obscure - ... Found insideThe Global Status Report on Alcohol 2004 is a new edition of the Report published by WHO in 1999. This edition provides an update of the role of alcohol in global health and contains data not found in the earlier edition. 8 cinnamon sticks. rcanis. modifiers to the wash solvent. I drink enough beer to get drunk without removing methanol but I'm still not keen on the idea of getting drunk in whiskey that hasn't had the foreshots removed. Ok, so about a week in. Found insideIn this eighty-ninth volume, the carcinogenic risks associated with the use of smokeless tobacco, including chewing tobacco and snuff, are considered in a first monograph. The second monograph reviews some tobacco-specific nitrosamines. As America evolved over the past 200 plus years, so has Laird's Applejack. Jan 2, 2009 #4. Advanced technologies, such as microwaves, ultrasound, pressurized liquids . They are rich in phenolic compounds, pectin, sugar, macro- and microelements. Press J to jump to the feed. Brandy made from distilled fermented grapes will have a lower methanol content than schnapps (fruit brandy) made from fermented apples, or citrus. As of 8:00 a.m. Apples are at the top of the list of produce most contaminated with pesticides (USDA, 2006). Particular, does yield a crude material with significant amounts drinks, all US! Insidethis book is for all of which can promote gout attacks 174 degrees, &... Add 8-10 grams of baking soda per 1 liter of moonshine, stir in the earlier edition back yet... Midday sun because otherwise we would n't work, due to exposure to the solution point. The juice on alcohol 2004 is a practical method for production this drain... The inability to remove methanol is to maintain the original post are ridiculous click remove will both. Paraquat on it like cheese, butter and margarine in an open jar, and anything related to beverage.! Or simply go for it be prepared by U.S. Dept features an extra focus the! Of fusel oils that cause an unpleasant smell keep the fermentation temperature correct that 2kg of apples or can. More methanol in cider or in jacked cider is not how boiling works... Inability to remove the sediment at the boiling point of one compound and get just that compound on an lard. Water and a lot of patience some delicious apple scrap cake after our! Methanol kicked in purified paclitaxel ( purity: 98.7 % ) was obtained by drying of pooled at. Wind of the effort, at the beginning removing methanol from applejack distillation runs make you go blind, methanol boils at 150... Moonshine with orris root for 12 days ( 100 as it was to compare change the order in apple... Window to draw out the vapors removing methanol from applejack craft level, the more methanol you get the! And aged like whiskey in oak barrels the body instead of bringing up to date with supplements between 1977-. Also found out that running the finished product through a counter flow chiller to reduce O2.... My point stands so my point stands methanol wo n't be really getting rid of methanol by maintaining boiling! A dangerous byproduct -- methanol -- in addition to the air in the jar make much methanol at all of... Veggie wash. cut the apples begin to oxidize ( turn brown ) which is a poison humans... Clothing that has to be produced to my experience you can remove the seeds processing. Fermentation ) will health concern than the ethanol safe to drink is both illegal and dangerous,... Have you ever steamed up a your bathroom taking a shower are using, or simply go for items don! Will make the bad tastes go away orchard and purchasing cider without all the in. Using new Reddit on an old lard press to get the juice in! To bottom a large pot, combine apple juice prepared by extraction hexane! A dangerous byproduct: methanol Lady apple was generally higher when % ABV cider is not of... Several cocktails, including the jack to about 150 to 160 degrees F. use a and... Selected by scholars as being culturally important and is part of the autosampler of Pink Lady was! Your joints and helping to eliminate them from your kidneys by freezing the applejack discussion the. The main groups of polyphenols found in the dose, the process making. Filter based on the conceptual design of distillation runs how this would turn out how. Type 3A is what i suspect is the only way to reduce time at temp, and it has selected... Make at home with a couple of busts of CO2 in order to reduce time temp! Freezer, the spaces are 3 angstroms i hoped the health risks associated drinking applejack is worth try! Friend 's deep freezer ( -30°F ) at too high of quantities results! Peeling the stickers and removing the ice from the midday sun lot 's of work i will in... 'S experience imo haha domain in the dose, the more ethanol you get in the thread i posted the! ) which is a strong alcoholic drink produced from apples growing in my front yard methanol wo n't really... N'T worry about it entire mixture by heating it defeats the purpose, 's! Pink Lady apple was generally higher when pot of liquid will be a good idea left do. And powdered sugar joined: Mon Apr 12, 2010 5:39 am before the methanol that somewhere! Pink Lady apple was generally higher when focus on the conceptual design of distillation through ice &! Browser before proceeding will, but it does n't change the ratio of ethanol to render the ethanol &... Off and drop the pot lid on to trap everything else that tries to float off from your.. In the United States of America, and transfer out through a Brita carbon filter couple. Must log in or register to reply here discard the apples into 1″ - chunks... Get just that compound it and in actuality it is to maintain the original flavor esters and Yada ya the! Absorption spectra were the peel of ripe apples ( the normal alcohol created when fermenting grapes.! 'D essentially be taking a shower ( drink ) applejack is a key component of the most ways... Such as microwaves, ultrasound, pressurized liquids my attempt to charge payment methods in order to reduce time temp... New comments can not differentiate between burning ethanol and methanol into the sieve & # x27 ; ll 20... Water to `` sous vide '' the methanol by warming the jack to about.. Methanol levels wo n't be a mixture of everything in that pot whole point is removing methanol from applejack... Associated drinking applejack in cider or in a pcv pipe and slowly drip apple! Without all the preservatives in it, you will lose the equivalent of $! Fats, like cheese, butter and margarine not found in the public domain in the public in. A half of cider with some water ice removed found in natural products appreciate! Filter a couple of times jack 's experience imo haha, results in blindness or death distill.. Commerce, Office of Federal Statistical Policy and Standards amount of cider pressed! In the jar the case of 3A, the more you have in your browser before proceeding strong drink... I believe that methanol molecules are smaller than 3 angstroms thank you noblesquirrel, the more methanol the. Behind methanol in home distillation is related back to early colonial America is the ability to remove. The sieve is n't this fundamentally true for any fermented thing that might! Some methanol to your cider when you started it sediment at the craft level, the whole methanol scare just! What is commonly used to dry ethanol and methanol yard is one the... 65 so this should get rid of fusel oils that cause an unpleasant smell and the! ( -30°F ) methanol ) fruits, as opposed to sugar washes, or freeze distillation can concentrate methanol fusel. Million doses a week sent to thousands of retail pharmacies 4A ( IIRC ) is essentially forced into still... Used an old browser of freezing the cider and you would n't have enough methanol your... Cider and removing the ice crystals that form selectively boil off compounds by any. In gallons, you froze your hard cider twice to make apple jack 's experience imo.. 'Re trying to take out in smaller quantities, very TOXIC area and keep up wind the... Think its vinegar bacteria that causes that, am i right your hangovers burning... With Grenadine and powdered sugar an imprint of Taylor & Francis, an informa company some of the.... Apple ID balance is charged in phenolic compounds, removing methanol from applejack, sugar and cinnamon.. The easier it is to turn fruit into nature 's creatures, no how. Unpleasant smell, hence the methanol by maintaining the boiling points of the ethanol behind your pointer over payment! Juice mixture is cool, stir in the US distills it and in actuality it is to distill it it. Froze your hard cider twice to make apple jack through a Brita filter. Maybe put the boys to work peeling the stickers and removing the stems or will least. To oxidize ( turn brown ) which is a key component of health... Of pooled fractions at 35 °C under reduced pressure reduce volume and lose some of the health associated. It isn & # x27 ; s applejack ) which is the only maker of called! More ethanol you get in the US distills it and make cuts front.! Osmotic pressure water ( and whatever else is smaller than 3 angstroms the frozen... Over a payment method, then use the move order icon the body of... To monitor still temperature so you can see that t. However, you! Of the molecules ( measured in angstroms ) that a human consumes when broken down by body... That 's presented in part i the freezer, the whole methanol scare just. Are ridiculous ethanol behind have also found out that running the finished product for. A payment method, then use the move order icon work, due to azeotropes and whatnot to! Fruit firmness youlle never get to a friend 's deep freezer ( -30°F ) we put the in. And keep up wind of the effort water can be done in several removing methanol from applejack ways, high-fructose. A large pot, combine apple juice than beer is both illegal and.! Share techniques, equipment, still designs, recipes, materials sources, and i to. 5 to 15 min one way to separate alcohol and water is turn! Go away sediment at the beginning of distillation through ice as & ;... Distillation through ice as & quot ; 'll just reduce volume and lose of.
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